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Solution State NMR Spectrometer 600MHz

Instrument types
NMR - Nuclear Magnetic Resonance
Make / Model : 
Varian Unity Inova 600 MHz
Instrument URL: 
More details about this Instrument

These spectrometers located in Chemistry and Biochemistry are equipped with multiple solution-state NMR probes for direct or indirect detection of 1H/19F and low frequency nuclei such as 13C, 31P, and 15N.

The 600MHz is also equipped with a cryoprobe. The state-of-the-art, cryogenically cooled probes provide significantly enhanced 1H and/or 13C sensitivity relative to room temperature probes, reducing experiment time up to 20 fold and making it possible for the detection of small-quantity of material. The high-field spectrometers along with the cryoprobes are ideal for biomolecular protein NMR. It is also being used for challenging small molecule projects, such as studies of low-quantity of natural products. 
 
5mm Varian triple resonance 1H/13C/15N inverse detection probe with Z-axis pulsed field gradient (PFG)
  • Temp: -20 to 80C
  • Four channels: 1H, 13C, 15N and lock (2H)
  • Best for 1H direct detection and indirect detection of 13C and 15N in 2D-4D NMR.
  • Autotuning not available.
Varian DBG600-5F 1H-19F/15N-31P with PFG, 5mm dual broadband
  • Temp: -80 to 120C
  • Three channels: 1H/19F, X and lock
  • Best for X nucleus (15N-31P) direct detection

 

Technical Primary Contact:
Hongjun Zhou

Access Procedure: 

All instruments are user operated and are open to all researchers and students with proper training. Instructions for training are the following link  http://nmr.chem.ucsb.edu/training/index.html. 

Training is offered throughout the year to prospective users in group sessions and mostly experiment or technique focused, hands-on individual sessions.